Process for making methyldichlorophosphane

Details Process for making methyldichlorophosphane Process for making methyldichlorophosphane

C - Chemistry, Metallurgy

07

F

260/537.6

C07F 9/48 (2006.01) C07F 9/52 (2006.01)

Patent

CA 1181090

PROCESS FOR MAKING METHYLDICHLOROPHOSPHANE ABSTRACT OF THE DISCLOSURE The disclosure relates to a process for making methyldi- chlorophosphane by reacting methane with phosphorus trichlo- ride in the presence of 2 to 7 mol% carbon tetrachloride, based on the phosphorus trichloride used, at temperatures of 500 to 650°C and over a period of time of 0.1 to 0.9 second. More particularly, the reaction is effected under a pressure of 2 to 10 bars, the proportion of carbon tetrachloride added being reduced at increasing pressure.

415680

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