Method of making large particle size, high purity dense silica

C - Chemistry – Metallurgy – 01 – B

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C01B 33/18 (2006.01) C01B 33/16 (2006.01) C03C 1/00 (2006.01)

Patent

CA 1318770

87-3-236 CN METHOD OF MAKING LARGE PARTICLE SIZE, HIGH PURITY DENSE SILICA Abstract: A method of making large particle size, high purity, dense silica is described. Tetraethylorthosilicate ethanol solution is added to a 2N ammonium hydroxide solution containing silicic acid having an average particle size of about 15 micrometers to form a precipitate followed by a digestion of the precipitate in the solution. The precipitate is filtered through a screen having 45 micrometer openings and dried to form a dried powder. The dried powder is then calcined in an oxygen atmosphere followed by desifying it by heating at a temperature of about 1200°C in air to form a large particle size, high purity, dense silica.

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