Solution process for preparing metal salt esters of...

C - Chemistry – Metallurgy – 07 – C

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C07C 69/593 (2006.01) C07C 67/00 (2006.01) C07C 67/08 (2006.01) C07C 69/34 (2006.01) C07C 69/40 (2006.01) C07C 69/52 (2006.01) C07C 323/12 (2006.01) C07F 3/04 (2006.01) C10M 129/95 (2006.01) C10M 135/24 (2006.01) C10M 135/26 (2006.01)

Patent

CA 1269399

Abstract of the Disclosure A solution process is disclosed for preparing a solubilized metal salt ester by reacting an ester compound, such as 2,2'-thiodiethyl-bis (octadecenyl) succinate ester, with a metal carboxylate, such as calcium acetate, in the presence of a mixture of (a) a first co-solvent and/or third co-solvent, such as toluene and/or dodecylbenzene respectively, and (b) a second co-solvent such as methanol, to form the metal salt ester product and an effluent mixture of an acid, such as acetic acid, optional co-solvent first, and second co-solvent, followed by the optional addition of a third co-solvent, and vacuum dis- tilling the resulting mixture to remove the effluent mixture to produce a solution of the product and third co-solvent.

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