Purification of n-methyl-2-pyrrolidone

C - Chemistry – Metallurgy – 07 – D

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C07D 207/267 (2006.01)

Patent

CA 1333806

A method for purifying N-methyl-2-pyrrolidone containing thiophenol and/or diphenyl disulfide is disclosed, comprising adding a polyhalogenated aromatic compound and an alkali metal hydroxide and/or an alkali metal carbonate to the N-methyl-2-pyrrolidone containing thiophenol and/or diphenyl disulfide, heat treating the mixture, and subjecting the mixture to separation by distillation. The thiophenol and/or diphenyl disulfide can be removed with ease and at low cost.

601619

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