Process for the preparation of organic azides

Details Process for the preparation of organic azides Process for the preparation of organic azides

C - Chemistry, Metallurgy

07

H

C07H 15/18 (2006.01) C07C 247/04 (2006.01) C07C 247/10 (2006.01) C07C 247/14 (2006.01) C07H 5/04 (2006.01)

Patent

CA 2296902

A process for the addition of an azide function to an organic compound in which process a mixture is prepared by adding an epoxide-derivative of the organic compound and an alkali metal azide salt to a solvent is described. The mixture is heated to a reaction temperature at which the epoxide-derivative and the azide can react to form an azide derivative of the organic compound. An amount, near equimolar to the epoxide derivative, of a (1-6C)alkyl-(2-- 4C)carboxylic acid ester having a boiling point above the reaction temperature is added to the mixture before and/or during the reaction.

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