Method for removing water from a mixture containing water...

C - Chemistry – Metallurgy – 01 – G

Patent

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Details

C01G 9/04 (2006.01) B01D 3/36 (2006.01) C07C 253/34 (2006.01) F26B 5/00 (2006.01) F26B 7/00 (2006.01)

Patent

CA 2491791

The invention relates to a method for removing water from a mixture containing water and zinc chloride. The invention is characterized in that said mixture containing water and zinc chloride is mixed with an aprotic, polar diluting agent whose boiling point, in the event of non-azeotropic formation of said diluting agent with water under the pressure conditions of the distillation mentioned below, is higher than the boiling point of water and is liquid at the boiling point of water or one azeotrope or heteroazeotrope with water is formed under the pressure and temperature conditions of the distillation mentioned below, and the mixture containing water, zinc chloride and the diluting agent is distilled while removing water or said azeotrope or said heteroazeotrope from this mixture while obtaining a water-free mixture containing zinc chloride and said diluting agent.

La présente invention concerne un procédé pour éliminer de l'eau d'un mélange qui contient de l'eau et du chlorure de zinc, qui se caractérise en ce que ledit mélange qui contient de l'eau et du chlorure de zinc est mélangé avec un agent de dilution polaire aprotique dont le point d'ébullition, dans le cas de la formation non azéotrope dudit agent de dilution avec de l'eau dans les conditions de pression de la distillation mentionnée ci-après, est supérieur au point d'ébullition de l'eau, et qui est présent à l'état liquide à ce point d'ébullition de l'eau, ou forme un azéotrope ou un hétéroazéotrope avec l'eau dans les conditions de pression et de température de la distillation mentionnée ci-après. Le mélange contenant de l'eau du chlorure de zinc et l'agent de dilution est alors distillé en même temps qu'a lieu la séparation de l'eau ou dudit azéotrope ou hétéroazéotrope, du mélange, pour obtenir un mélange dépourvu d'eau contenant du chlorure de zinc et ledit agent de dilution.

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