Production of recombinant interferon proteins

C - Chemistry – Metallurgy – 12 – N

Patent

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C12N 5/10 (2006.01) C07K 1/18 (2006.01) C07K 14/555 (2006.01) C07K 14/56 (2006.01) C12N 15/85 (2006.01) C12P 21/02 (2006.01)

Patent

CA 2708291

A method of purifying a recombinant interferon protein involves providing an aqueous mixture of the recombinant protein and contaminating proteins; precipitating the contaminating proteins from the aqueous mixture at a pH in a range of from 0.5 to 6; separating the aqueous mixture from the precipitated contaminating proteins; and, eluting the separated aqueous mixture through a cation exchange column using a mobile phase with a salt or pH gradient, the gradient being from lower salt concentration or pH to higher salt concentration or pH, to produce a recombinant interferon protein fraction separated from other components of the aqueous mixture. The method provides for the recovery of recombinant interferon proteins in better yield and purity.

L'invention concerne un procédé de purification d'une protéine interféron de recombinaison, consistant à former un mélange aqueux contenant la protéine de recombinaison et des protéines de contamination; à précipiter les protéines de contamination du mélange aqueux à un pH variant entre 0,5 et 6; à séparer le mélange aqueux des protéines de contamination précipitées; et à éluer le mélange aqueux séparé dans une colonne d'échange de cations à l'aide d'une phase mobile avec un gradient de sel ou de pH, le gradient présentant une concentration en sel ou pH inférieurs ou une concentration en sel ou pH supérieurs, afin d'obtenir une fraction de protéine interféron séparée des autres composants du mélange aqueux. Le procédé permet la récupération des protéines interférons de recombinaison avec un rendement et une pureté supérieurs.

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