Preparation of esters of thiocarbamic acids involving use of...

C - Chemistry – Metallurgy – 07 – D

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260/241.54, 260/

C07D 295/20 (2006.01) A01N 47/10 (2006.01) A01N 47/12 (2006.01) A01N 47/18 (2006.01) C07D 295/21 (2006.01)

Patent

CA 1103665

\ Abstract of the Disclosure Ester of thiocarbamic acids are prepared by a process comprising (a) reacting a carbamyl chloride with a mercaptan in the presence of (i) an aqueous solution of a caustic agent, and (ii) a catalytic amount of a phase transfer catalyst; (b) separating the organic ant aqueous phases; and (c) recovering the thiocarbamic acid enter from the organic phase

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