C - Chemistry – Metallurgy – 07 – D
Patent
C - Chemistry, Metallurgy
07
D
260/364.8
C07D 307/89 (2006.01) C07C 2/86 (2006.01) C07C 51/275 (2006.01) C07C 51/56 (2006.01)
Patent
CA 1117959
PROCESS FOR PREPARING 3,4,3',4-BENZOPHENONETETRA- CARBOXYLIC DIANHYDRIDE ABSTRACT OF THE DISCLOSURE A process for preparing 3,4,3',4'-benzophenonetetra- carboxylic dianhydride which comprises condensing an impure ortho-xylene mixture with acetaldehyde in contact with an acid catalyst to obtain an impure 1,1-bis(3,4-dimethylphenyl)ethane mixture, oxidizing the 1,1-bis(3,4-dimethylphenyl)ethane mixture with nitric acid to obtain a mixture of carboxylic acids, from which by crystallization and dehydration substantially pure 3,4,3',4'-benzophenonetetracarboxylic dianhydride is recovered.
330492
Onopchenko Anatoli
Schulz Johann G. D.
Gulf Research & Development Company
Mccarthy Tetrault Llp
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