Process for the recovery of a water-insoluble epoxy alcohol

Details Process for the recovery of a water-insoluble epoxy alcohol Process for the recovery of a water-insoluble epoxy alcohol

C - Chemistry, Metallurgy

07

D

202/101, 260/374

C07D 301/32 (2006.01) B01D 3/10 (2006.01) C07D 303/14 (2006.01)

Patent

CA 2025746

Water-insoluble crystallizable epoxy alcohols such as phenyl glycidol are recovered from epoxidation reaction mixtures by washing the mixture with water, concentrating the mixture by distillation under vacuum to remove unreacted hydroperoxide and alcohol co-product, and crystallizing the epoxy alcohol from solution. Minimal decomposition of the epoxy alcohol is observed.

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