Use of nuclear magnetic resonance to identify ligands to...

G - Physics – 01 – N

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G01N 24/08 (2006.01) C12Q 1/00 (2006.01) C12Q 1/37 (2006.01) C12Q 1/68 (2006.01) G01R 33/465 (2006.01) C40B 30/04 (2006.01)

Patent

CA 2237343

The present invention provides a process for identifying compounds which bind to a specific target molecule. The process includes the steps of: a) generating a first two-dimensional 15N/1H NMR correlation spectrum of a 15N-labeled target molecule; b) exposing the labeled target molecule to one or a mixture of chemical compounds; c) generating a second two-dimensional 15N/1H NMR correlation spectrum of the labeled target molecule that has been exposed to one or a mixture of compounds in step (b); and d) comparing said first and second two-dimensional 15N/1H NMR correlation spectra to determine differences between said first and said second spectra, the differences indentifying the presence of one or more compounds that are ligands which have bound to the target molecule.

La présente invention concerne un procédé pour identifier des composés se liant à une molécule cible spécifique. Ce procédé consiste à: (a) créer un premier spectre de corrélation bidimensionnel <15>N/<1>H NMR d'une molécule cible marquée <15>N; b) exposer la molécule cible marquée à un composé ou à un mélange de composés chimiques; c) créer un deuxième spectre de corrélation bidimensionnel <15>N/<1>H NMR de la molécule cible marquée qui a été exposée à un composé ou à un mélange de composés lors de l'étape (b); et d) comparer lesdits premier et deuxième spectres de corrélation bidimensionnels <15>N/<1>H NMR en vue de déterminer les différences entre ces premier et deuxième spectres, ces différences identifiant la présence d'un ou de plusieurs composés qui sont des ligands s'étant liés à la molécule cible.

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