Process for the hydroformylation of ethylenically...

C - Chemistry – Metallurgy – 07 – C

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C07C 29/16 (2006.01)

Patent

CA 2510165

The invention pertains to a process for the hydroformylation of an ethylenically unsaturated compound in the presence of an acid with a pKa < +3, and a catalyst of a group VIII metal and a bidentate ligand of the formula: R1R2-P-X-P-R3R4 (I) wherein P is a phosphorus atom, X represents a bivalent organic bridging group, R1, R2, R3 and R4 represent independently a substituted or unsubstituted hydrocarbyl group, or R1 and R2 together with the phosphorus atom to which they are bonded and/or R3 and R4 together with the phosphorus atom to which they are bonded represent a bivalent substituted or unsubstituted cyclic group, characterized in that the process is performed in the presence of a mono tert-phosphine, wherein the ratio moles of mono tert- phosphine : moles of acid is from 1 : 1 to 10 : 1.

L'invention concerne un procédé pour l'hydroformylation d'un composé éthylénique insaturé en présence d'un acide avec un pKa < +3, et un catalyseur d'un métal de groupe VIII et un ligand bidenté de formule R¿1?R¿2?-P-X-P-R¿3?R¿4? (I), dans laquelle P représente un atome de phosphore, X représente un groupe de pontage organique bivalent, R¿1?, R¿2?, R¿3? et R¿4? représentent indépendamment un groupe hydrocarbyle substitué ou non substitué, ou R¿1? et R¿2? avec l'atome de phosphore auquel ils sont liés et/ou R¿3? et R¿4? avec l'atome de phosphore auquel ils sont liés représentent un groupe cyclique substitué ou non substitué bivalent. Ce procédé se caractérise en ce qu'il est réalisé en présence d'une mono tert-phosphine, le rapport moles de mono tert-phosphine: moles d'acide étant compris entre 1: 1 et 10 : 1.

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