Spectroscopy-based real-time control for microwave-assisted...

Details Spectroscopy-based real-time control for microwave-assisted... Spectroscopy-based real-time control for microwave-assisted...

B - Operations, Transporting

01

J

B01J 19/12 (2006.01) G01N 21/65 (2006.01)

Patent

CA 2541485

The invention is an instrument and method for microwave-assisted chemical synthesis. The instrument includes a source of microwave radiation for applying microwave energy to a sample, a microwave cavity in wave communication with the source for holding the sample during the application of microwave energy, and a substantially monochromatic radiation source in electromagnetic communication with the cavity for applying substantially monochromatic light to the sample. The instrument further includes a detector positioned to detect Raman scattering of light from the monochromatic source by the sample, and a controller in signal communication with the microwave energy source and the Raman scattering detector for moderating the application of microwave energy to the sample based upon the detected Raman scattering.

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