Assay for determining the activity of fatty acid amide...

C - Chemistry – Metallurgy – 12 – Q

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C12Q 1/34 (2006.01) B01D 1/00 (2006.01) G01N 33/92 (2006.01)

Patent

CA 2503078

The invention provides methods of assaying fatty acid amide hydrolase (FAAH) activity adaptable for high throughput screening. The methods provide for separating a labeled substrate from at least one labeled hydrolysis product, the separation facilitating the quantification. The invention also provides methods of identifying a compound to be tested as an inhibitor or an activator of FAAH activity through the addition of the compound to be tested to a reaction mixture and comparison of the enzyme activity in the presence and absence of the compounds to be tested. The methods are adaptable for use in detecting altered FAAH activity in patients, for example, those at risk for in vitro fertilization failure, or at risk for, or suffering, addictions.

L'invention concerne des méthodes d'analyse de l'activité de l'hydrolase des amides d'acides gras (FAAH) adaptées à un criblage à haut débit. Ces méthodes consistent à séparer un substrat marqué d'au moins un produit d'hydrolyse marqué, cette séparation facilitant la quantification. L'invention concerne également des méthodes destinées à identifier un composé à tester en tant qu'inhibiteur ou activateur de l'activité de la FAAH par addition du composé à tester dans un mélange de réaction et par comparaison de l'activité enzymatique en présence et en absence des composés à tester. Lesdites méthodes peuvent être adaptées à une utilisation dans la détection d'une activité FAAH modifiée chez des patients, tels que ceux présentant un risque d'échec de fécondation in vitro ou ceux risquant de présenter ou présentant des dépendances.

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