C - Chemistry – Metallurgy – 09 – K
Patent
C - Chemistry, Metallurgy
09
K
C09K 11/01 (2006.01)
Patent
CA 2363391
A method of recovering a base phosphor from encapsulated phosphors, which comprises the steps of selecting a recovery vessel including a magnetic stir bar; adding to the recovery vessel, deionized water, a first batch of concentrated hydrochloric acid and encapsulated phosphor to form a stirred suspension; heating the stirred suspension to about 90°C for about 2 hours; settling the stirred suspension; decanting the mother liquor and slurrying the remaining solids with a second batch of hydrochloric acid and water; decanting and washing the remaining solids with deionized water; filtering the remaining solids to form a filter cake; heating the filter cake at 110°C in air for a time sufficient to form a dried filter cake; and screening the dried filter cake through a -325 mesh screen to yield a recovered base phosphor.
Fan Chen-Wen
Gingerich Richard G.w.
Klinedinst Keith A.
Fetherstonhaugh & Co.
Osram Sylvania Inc.
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