Process for the preparation of 1,5,-imino, -1,5,6-trideoxy...

Details Process for the preparation of 1,5,-imino, -1,5,6-trideoxy... Process for the preparation of 1,5,-imino, -1,5,6-trideoxy...

C - Chemistry, Metallurgy

07

D

C07D 211/40 (2006.01) C07H 5/06 (2006.01)

Patent

CA 2521029

The invention comprises a process for the preparation of 1,5-imino,-1,5,6-trideoxy hexitol. The process comprises reacting methyl-2,3,4,6-tetra-O-acetyl-5- hexulosonic acid oxime with hydrogen and a hydrogenation catalyst to form a 1, 5, 6-triacetoxy acid lactam and reducing and deacetylating the lactam with a reducing agent to form the 1,5-imino hexitol. The invention also comprises tri-O- acetyl-5-amino-5,6-dideoxy-D-gluconic acid lactam.

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