Assay for phosphatase-targeting toxins

C - Chemistry – Metallurgy – 12 – Q

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Details

C12Q 1/42 (2006.01) G01N 33/53 (2006.01)

Patent

CA 2349942

The invention provides an assay method for determining phosphatase targeting toxins which inhibit protein phosphatases comprising contacting a solid support having an immobilized ligand immobilized thereon with: (i) a sample suspected of being contaminated with toxin and (ii) a non-immobilized ligand, wherein said immobilized ligand is capable of generating directly or indirectly detectable signal when uncomplexed, when complexed by said toxin, when complexed by a complex of said toxin and said non-immobilized ligand or when complexed by said non-immobilized ligand or said non-immobilized ligand is capable of generating a directly or indirectly detectable signal when uncomplexed or when complexed, separating a bound fraction from a non-bound fraction; and directly or indirectly determining the non-immobilized ligand bound to the immobilized ligand (the bound fraction) or non-complexed in aqueous solution (the non-bound fraction).

L'invention concerne un procédé de dosage permettant de déterminer les toxines de ciblage de phosphatase qui inhibent les phosphatases protéiques. Ce procédé consiste à placer en contact un support solide sur lequel est immobilisé un ligand avec (i) un échantillon suspecté d'être contaminé par une toxine et (ii) un ligand non immobilisé. Ledit ligand peut générer directement ou indirectement un signal pouvant être détecté lorsqu'il est complexé ou non par ladite toxine, complexé par un complexe de ladite toxine et dudit ligand non immobilisé, ou complexé par ledit ligand non immobilisé. Ledit ligand non immobilisé peut générer un signal pouvant être directement ou indirectement détecté lorsqu'il est complexé ou non complexé, en séparant une fraction liée d'une fraction non liée et en déterminant directement, ou indirectement, le ligand non immobilisé lié au ligand immobilisé (fraction liée) ou non complexé dans une solution aqueuse (fraction non liée).

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