Bisulfite purification of an alpha-keto amide

Details Bisulfite purification of an alpha-keto amide Bisulfite purification of an alpha-keto amide

C - Chemistry, Metallurgy

07

D

C07D 209/52 (2006.01)

Patent

CA 2672268

A process for purifying the alpha-keto amide is (1R,5S)-N-[3-amino-1-(cyclobutylmethyl)-2,3-dioxopropyl]-3-[2(S)-[[[(1,1-dimethylethyl)amino]carbonyl]-amino]-3,3-dimethyl-1-oxobutyl]-6,6-dimethyl-3-azabicyclo[3.1.0]hexan-2(S)-carboxamide via a bisulfite adduct is disclosed.

La présente invention concerne un procédé de purification d'un alpha-céto-amide qui est le (1R,5S)-N-[3-amino-1-(cyclobutylméthyl)-2,3-dioxopropyl]-3-[2(S)-[[[(1,1-diméthyléthyl)amino]carbonyl]amino]-3,3-diméthyl-1-oxobutyl]-6,6-diméthyl-3-azabicyclo[3.1.0]hexane-2(S)-carboxamide à l'aide d'un produit d'addition de bisulfite.

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