Process for the removal of nitrosation agent(s) from...

C - Chemistry – Metallurgy – 07 – D

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260/557.4, 260/6

C07D 217/24 (2006.01) C07D 209/46 (2006.01)

Patent

CA 1133014

ABSTRACT OF THE DISCLOSURE Nitrated aromatic compounds with a solidification point of more than about 10°C are obtained from the nitration batch without separation of the aqueous phase by crystalli- zation in a form practically without nitrosation agents. 4-Chloro-3,5-dinitrobenzotrifluoride, for example, which has been crystallized in this way, yields a Trifluralin, which has a nitrosamine content of a maximum of about 1 ppm upon further reaction with di-n-propylamine.

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