Process for preparing n-trimethylsilylacetamide

Details Process for preparing n-trimethylsilylacetamide Process for preparing n-trimethylsilylacetamide

C - Chemistry, Metallurgy

07

F

260/446.3

C07F 7/02 (2006.01) C07F 7/10 (2006.01)

Patent

CA 1039737

ABSTRACT The invention provides a process for preparing N-trimethylsilylacetamide by reacting hexamethyldisilazane with acetamide in a ratio of at least one mole of hexamethyl- disilazane per each two moles of acetamide at a temperature of from about 40°C. to about 125°C. for the period of time during which ammonia is generated from the mixture, and continuously removing the ammonia from the mixture during the period of its generation.

211680

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