C - Chemistry – Metallurgy – 04 – B
Patent
C - Chemistry, Metallurgy
04
B
25/133, 25/140
C04B 35/58 (2006.01) C04B 35/593 (2006.01)
Patent
CA 1142333
-10- ABSTRACT OF THE DISCLOSURE A method of making a unitary silicon nitride comprising object is disclosed. A uniform powder mixture is prepared of Si3N4 containing SiO2 as an oxide surface coating, 4-12% by weight Y2O3, and .50-2.5% Al2O3. The mixture is heated to 1000-1400°C under a pressure of at least 2,000 psi for a time of at least one minute but sufficient to permit a nucleating reaction to take place in secondary phases. Heating is then increased to a temperature of 1680-1750°C under a pressure and for a period of time sufficient to produce 99.0% or more of full theoretical density in the pressed object.
359892
Ezis Andre
Ford Motor Company Of Canada Limited
Sim & Mcburney
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