Process for filled diorganopolysiloxane elastomers

C - Chemistry – Metallurgy – 08 – L

Patent

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400/4104, 400/53

C08L 83/04 (2006.01)

Patent

CA 1069241

ABSTRACT OF THE DISCLOSURE An improved process is provided for preparing compositions capable of being converted into elastomers. The compositions are ones containing (A) triorganosiloxy-terminated diorganopoly- siloxanes having at least one vinyl group in each terminal units, (B) triorganosiloxy-terminated organopolysiloxanes containing organonydrogensiloxane units and diorganosiloxane units, (C) fillers, which are hydrophobic or are capable of being rendered hydrophobic and having a surface area of at least 50 m2/g and (D) catalysts which promote the addition of SiH groups to vinyl groups, and preferably also diorganopolysiloxanes (E) having on the average for each molecule, as terminal units, two diorgano- hydrogensiloxane units of the formula R2HSio1/2 or one diorganohydrogensiloxane unit of the formula R2HSi01/2 and one CH2=CR2SiO1/2 unit. The improved process comprises the essential steps of mixing organopolysiloxanes (B) containing organo- hydrogensiloxane (SiH) units with at least 75 percent by weight of the fillers (C) having a surface area of at least 50 m2/g before mixing with the organopolysiloxanes (A) having tri- organosiloxy-terminated units with at least one vinyl group in each terminal unit. The compositions are capable of being poured and/or brushed. The elastomers provided have improved tensile strength and tear resistance, are smooth and substantially free of gas bubbles, and have better mechanical properties than those of the prior art.

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