2-hydroxymethyl-3-hydroxy-6-(1-hydroxy-2-t-butylaminoethyl)...

Details 2-hydroxymethyl-3-hydroxy-6-(1-hydroxy-2-t-butylaminoethyl)... 2-hydroxymethyl-3-hydroxy-6-(1-hydroxy-2-t-butylaminoethyl)...

C - Chemistry, Metallurgy

07

D

260/297

C07D 213/66 (2006.01) C07D 213/65 (2006.01)

Patent

CA 1074322

ABSTRACT OF THE DISCLOSURE Hydrogenolysis of the benzylidene acetal 2-phenyl-6- (1-hydroxy-2-t-butylaminoethyl)-4H-pyrido[3,2-d]-1,3-dioxin to the free base, 2-hydroxymethyl-3-hydroxy-6-(1-hydroxy-2-t-butyl- aminoethyl)pyridine especially in the presence of water, and conversion of the base to acid addition salts, especially the acetate salt.

302314

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