A method for preparing a cellulose ether

C - Chemistry – Metallurgy – 08 – B

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C08B 11/00 (2006.01) C08B 11/12 (2006.01)

Patent

CA 2548007

The invention relates to a method for preparing a cellulose ether. The method comprises mixing cellulose with an ionic liquid solvent to dissolve the cellulose, and then treating the dissolved cellulose with an etherifying agent in the presence of an inorganic base to form a cellulose ether, and subsequently separating the cellulose ether from the solution, wherein both the dissolution and the etherification are carried out in the absence of an organic base and in the substantial absence of water. Microwave irradiation and/or pressure can be applied to assist in dissolution and etherification.

L'invention concerne une méthode de préparation d'un éther cellulosique. Cette méthode consiste à mélanger de la cellulose et un solvant liquide ionique pour dissoudre la cellulose, puis à traiter la cellulose dissoute à l'aide d'un agent d'étherification, en présence d'une base inorganique, pour former un éther cellulosique, et ensuite à séparer l'éther cellulosique de la solution, la dissolution et l'étherification étant toutes deux effectuées en l'absence d'une base organique, et en l'absence sensible d'eau. Le rayonnement de micro-ondes et/ou la pression peuvent être appliqués pour faciliter la dissolution et l'étherification.

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