C - Chemistry – Metallurgy – 07 – F
Patent
C - Chemistry, Metallurgy
07
F
C07F 9/17 (2006.01)
Patent
CA 2073737
Stable S,S,S-tributylphosphorotrithioate having reduced levels of the odorous by-product dibutyl disulfide is produced by adding a caustic solution having a concentration of less than 10% to crude S,S,S-tributylphosphorotrithioate until the pH remains constant. In a preferred embodiment, a solution of sodium hydroxide having a concentration of less than 10% is used in an amount such that at least 0.1 mole of sodium hydroxide is present for each mole of crude S,S,S-tributylphosphortrithioate.
Levy Edward R.
Newallis Peter E.
Prasad Vidyanatha A.
Corporation Bayer
Miles Inc.
Norton Rose Or S.e.n.c.r.l. S.r.l./llp
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