A process for removing pyrophoric catalyst

B - Operations – Transporting – 01 – J

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B01J 8/00 (2006.01) B01D 29/27 (2006.01) B01J 25/04 (2006.01) C07B 31/00 (2006.01)

Patent

CA 2389561

A batch process for carrying out a hydrogenation reaction comprises mixing a pyrophoric catalyst with reactants and solvents to form a reaction mixture in a reaction vessel. Hydrogen is added to the reaction vessel. After hydrogenation, the desired hydrogenation product is removed from the reaction vessel and the pyrophoric catalyst-rich material from the reaction vessel is delivered to a pressure filter. Water is added to the pyrophoric catalyst-rich material in the filter and the spent pyrophoric material is removed from the pressure filter in a water wet form.

L'invention concerne un procédé discontinu permettant d'effectuer une réaction d'hydrogénation et consistant à mélanger un catalyseur pyrophorique avec des réactifs et des solvants afin de former un mélange de réaction dans une cuve de réaction. On ajoute de l'hydrogène à la cuve de réaction. Après l'hydrogénation, on enlève le produit d'hydrogénation voulu de la cuve de réaction et la matière riche en catalyseur pyrophorique de la cuve de réaction est amenée dans un filtre sous pression. Dans le filtre, on ajoute de l'eau à cette matière riche en catalyseur pyrophorique, puis la matière pyrophorique usée est éliminée du filtre sous pression sous une forme humide.

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