A process for the preparation of...

C - Chemistry – Metallurgy – 07 – C

Patent

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C07C 33/048 (2006.01) C07C 29/42 (2006.01) C07C 29/44 (2006.01)

Patent

CA 2350394

The invention provides a process for the preparation of 6,6-dimethylhept-1-en-4-yn-3-of comprising of reacting t-butylacetylene with a proton-extracting agent selected from the group consisting of an organometallic compound and metallic lithium to form a t-butylacetylide, reacting the acetylide with acrolein at temperatures between -40°C to +20°C, quenching the reaction mixture and isolating the product.

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