A process for the preparation of high-purity organosilicon...

C - Chemistry – Metallurgy – 07 – F

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C07F 7/08 (2006.01) C07F 7/18 (2006.01)

Patent

CA 2244597

The preparation of high-purity organosilicon disulphanes in which, in a two-stage process, elemental sulphur and an anhydrous alkali sulphide in a deficient amount is first reacted with a halogen alkylalkoxysilane, and the sulphur deficit is then made up by the addition of further alkali sulphide.

Préparation en deux étapes de disulphanes organosiliciés de grande pureté, consistant à faire réagir d'abord du soufre élémentaire et un sulfure d'alcali anhydre en quantité déficitaire avec un alkylalcoxysilane halogéné; le déficit en sulfure est ensuite comblé par addition de sulfure d'alcali supplémentaire.

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