Adiabatic calorimeter apparatus and method for measuring the...

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73/100, 73/123,

G01N 25/48 (2006.01) G01K 17/00 (2006.01) G01N 25/22 (2006.01)

Patent

CA 1089671

ABSTRACT OF THE DISCLOSURE An adiabatic calorimeter apparatus disclosed herein is designed for determining the chemical hazard in exothermic or high energy chemical reactions which can result in hazardous runaway reactions and under extreme conditions in an explosion of the reactants. The reaction vessel is suspended in an insulated chamber. During the exothermic reaction the adiabatic temperature rise and pressure rise is simultaneously monitored and recorded as a function of time. A first stage control system maintains the temperature of the reaction vessel in equi- librium with the reaction mix to utilized s conductive electrical resistance heater to heat the reaction vessel to compensate for the heat content (the heat capacity or specific heat multiplied by the mass of the reaction vessel) of the reactor. The reaction vessel and asso- ciated components in this apparatus closely simulate the structure and operation of a typical chemical plant reactor.

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