Alkylation of substituted sulfonylpyridine 1-oxides

C - Chemistry – Metallurgy – 07 – D

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260/290.3, 260/2

C07D 213/70 (2006.01) C07D 213/71 (2006.01) C07D 213/89 (2006.01)

Patent

CA 1163997

ABSTRACT Making a compound of the formula Image ( I ) wherein: R is Cl-C12 al? yl, allyl or benzyl, R1 and R2 are hydrogen, halogen, Cl-C4 alkyl, or phenyl, R3 is hydrogen, halogen, Cl-C4 alkyl, C1-C4 alkoxy, CF3, N02, phenyl or phenoxy m is an integer from 1 to 3 and n is zero or 1, by contacting a compound Or said formula where R is hydrogen with certain halohydrocarbons in the presence of solid KOH, a phase transfer catalyst, a solvent and an effective amount of water.

396036

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