Amide forming chemical ligation

Details Amide forming chemical ligation Amide forming chemical ligation

C - Chemistry, Metallurgy

07

C

C07C 233/02 (2006.01)

Patent

CA 2615032

An amide is formed by reacting an .alpha.-ketoacid or salt thereof in a decarboxylative condensation reaction with an amine or salt thereof comprising a nitrogen covalently bound to an atom selected from oxygen, nitrogen, and sulfur. The amide bond is formed between the .alpha.-carbon of the ketoacid and the nitrogen of the amine. The .alpha.-ketoacid can be formed using a novel sulfur reagent.

L~invention concerne la formation d~un amide par réaction d~un .alpha.-cétoacide ou d~un sel d~un .alpha.-cétoacide par une réaction de condensation décarboxylative avec une amine ou un sel d~une amine comprenant un azote lié par une liaison covalente à un atome choisi parmi l~oxygène, l~azote et le soufre. La liaison amide est formée entre l~.alpha.-carbone du cétoacide et l~azote de l~amine. L~.alpha.-cétoacide peut être formé en utilisant un nouveau réactif à base de soufre.

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