Catalytic oxidation of 3,3-dimethyl 2-hydroxybutyric acid to...

C - Chemistry – Metallurgy – 07 – C

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260/248.6, 260/5

C07C 59/185 (2006.01) C07C 51/373 (2006.01) C07D 253/06 (2006.01)

Patent

CA 1113936

Abstract of the Disclosure Sodium 3,3-dimethyl-2-hydroxybutyrate and ruthenium dioxide hydrate are added to water, the pH rendered alkaline, and sodium hypochlorite is slowly added to produce sodium 3,3-dimethyl-2-oxybutyrate in high yield and purity. The solid catalyst is filtered off and may be re-used while the filtrate can be directly used in further synthesis.

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