Chlorinator furnace and method for producing tetrachloride...

C - Chemistry – Metallurgy – 01 – G

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C01G 23/02 (2006.01) C01G 25/04 (2006.01) C22B 1/08 (2006.01) C22B 34/12 (2006.01) C22B 34/14 (2006.01) F27B 15/00 (2006.01)

Patent

CA 1179827

ABSTRACT OF THE DISCLOSURE A chlorinator furnace for producing tetrach]oride of such metal as titanium ? zirconium, comprising: a wall structure substantially consisting of refractory material which provides inside a vertically elongated reaction chamber which, in turn, includes a substantially cylindrical reaction zone ranging down from an intermediate level of the reaction chamber, an encasement of iron sheet to cover a substantial part of said wall structure, a duct -eans for exhausting gases, connected to said reaction chamber at an upper portion thereof, a tube means for supplying regulated flow of gases containing chlorine, connected to the reaction chamber at a bottom thereof, a pipe means for introducing solid materials into the reaction zone, extending through the encasement and wall structure and provided with pressure regulating means, a jacket means which is provided as adjacent to the wall structure and capable of holding a gas harmless to the reaction inside the chamber at a somewhat raised pressure over the atmosphere, said jacket means axially extending around the chamber so as to cover at least the reaction zone, and a means for regulating a pressure in the jacket within a given range, and a method for producing tetra- chloride of such metal as titanium and zirconium.

400487

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