Combinational method for microgram-scale production and...

B - Operations – Transporting – 01 – J

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B01J 19/00 (2006.01) B01J 3/04 (2006.01) B01L 3/00 (2006.01) C07B 61/00 (2006.01)

Patent

CA 2333178

The invention relates to a method for wet chemical production of a plurality of libraries of materials consisting of solids, whereby the solids are separated from reaction mixtures in microreaction chambers on a base plate serving at the same time as substrate for the library. Depending on the material chosen for the substrate of the library, solids can be subsequently investigated in a non-destructive manner, e.g. by means of reflecting or penetrating microarea x-ray scattering. Preferably, the reactor consists of a cylindrical pressurized container made of steel having a silicon monocrystal plate as library. A steel plate with tetrafluoroethylene coating is pressed on said Si-monocrystal plate by means of screws, the holes of which form the reaction chambers.

L'invention concerne un procédé pour produire de manière chimique par voie humide des bibliothèques de matériaux comprenant une pluralité de matières solides, ces dernières étant séparées des mélanges réactionnels dans des chambres de microréaction sur une plaque de base qui sert également de substrat de bibliothèque. En fonction du choix du matériau pour le substrat de bibliothèque, les matières solides peuvent ensuite être analysées de manière non destructive, par exemple par dispersion de rayons X, de l'ordre du micron, qui sont réfléchis par la plaque de base ou pénètrent dans cette dernière.

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