Continuous preparation of dialkanesulfonyl peroxide

Details Continuous preparation of dialkanesulfonyl peroxide Continuous preparation of dialkanesulfonyl peroxide

C - Chemistry, Metallurgy

25

B

204/53

C25B 3/02 (2006.01) C25B 3/10 (2006.01)

Patent

CA 1305097

ABSTRACT Dialkanesulfonyl peroxide (RSO2-O-O-O2SR) is prepared in a continuous process by electrolyzing the corresponding alkanesulfonic acid at an elevated temperature (to keep the peroxide product in solution) in a continuous-flow electrolysis cell, removing the solution from the electrolytic cell, cooling the solution to precipitate the peroxide product, and recycling the supernatant alkanesulfonic acid back to the cell.

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