Continuous process for producing nitrilotriacetonitrile

B - Operations – Transporting – 01 – J

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260/561.3

B01J 19/24 (2006.01)

Patent

CA 1205090

ABSTRACT CONTINUOUS PROCESS FOR PRODUCING NITRILOTRIACETONITRILE A continuous process for preparing hitrilotriacetonitrile in which the reactants, formaldehyde, hydrogen cyanide, and either am- monia or hexamethylenetetramine are reacted first in a mixing reactor, preferably a circulating loop reactor at from about 90°C to about 120°C, then reacted in a plug flow tubular reactor at from about 95°C to about 120°C, then after cool- ing the reaction mixture crystalline nitrilotri- acetonitrile is recovered.

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