Continuous process for the production of dichloroacetamides

Details Continuous process for the production of dichloroacetamides Continuous process for the production of dichloroacetamides

C - Chemistry, Metallurgy

07

D

260/556.3, 260/3

C07D 263/04 (2006.01) C07C 103/365 (1980.01)

Patent

CA 1157867

Abstract of the Invention Dichloroacetylamides selected from the group consisting of: a) N,N-diallyldichloroacetamide, and b) N-dichloroacetyl oxazolidines having the formula Image in which R is hydrogen or C1-C3 alkyl are produced in a continuous circulating process by reaction of dichloroacetyl chloride with respectively N,N- diallylamine or an oxazolidine having the formula Image in the presence of an aqueous solution of sodium hydroxide. The conduct of this process in a con- tinuous circulating fashion produces the desired amide in greater yield than by the heretofore practiced batch processes.

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