C - Chemistry – Metallurgy – 07 – D
Patent
C - Chemistry, Metallurgy
07
D
C07D 307/12 (2006.01)
Patent
CA 2590123
A method of preparing 2,5-bis(hydroxymethyl)tetrahydrofuran comprises heating a reaction mixture comprising 2,5-(hydroxymethyl)furaldehyde, an organic solvent, and a catalyst system comprising nickel and zirconium at a temperature, for a time, and at a pressure sufficient to promote reduction of the 2,5-(hydroxymethyl)furaldehyde to 2,5-bis(hydroxymethyl)tetrahydrofuran to produce a product mixture comprising 2,5-bis(hydroxymethyl)tetrahydrofuran.
La présente invention a trait à un procédé de préparation de 2,5-bis(hydroxyméthyl)tétrahydrofuranne comprenant le réchauffement d'un mélange réactionnel comportant du 2,5-(hydroxyméthyl)furaldéhyde, un solvant organique, et un système catalytique comprenant du nickel et du zirconium à une température, pour une durée, et à une pression suffisantes pour favoriser la réduction du 2,5-(hydroxyméthyl)furaldéhyde en 2,5-bis(hydroxyméthyl)tétrahydrofuranne en vue de produire un mélange de produit comprenant du 2,5-bis(hydroxyméthyl)tétrahydrofuranne.
Bloom Paul D.
Sanborn Alexandra J.
Archer-Daniels-Midland Company
Ridout & Maybee Llp
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