Cryogenic apparatus

F - Mech Eng,Light,Heat,Weapons – 25 – D

Patent

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Details

F25D 3/11 (2006.01) A23L 3/375 (2006.01) B01J 19/06 (2006.01) F25C 1/00 (2006.01) F26B 5/06 (2006.01) G01N 1/42 (2006.01)

Patent

CA 2134224

The present invention provides methods and devices for freezing drops of liquid reagent solutions in a cryogenic liquid. In one embodiment, the apparatus of the present invention comprises mans for dispensing (22) uniform, precisely measured drops of a liquid reagent (4) and a rotatable carousel (36) positioned below the dispensing means (22). The upper surface of the carousel has a plurality of trays (58) each containing a cryogenic liquid, typically liquid nitrogen, for receiving the drops of liquid reagent. An alternative embodiment of the present invention comprises a tank (66) comprising a cryogenic liquid for receiving the drops of liquid reagent. The tank has a heat source (70) for slightly heating a portion of the cryogenic liquid such that a convection current in the cryogenic liquid provide mild agitation of the liquid and prevent aggregation of the frozen drops.

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