Crystal flux synthesis and epitaxy of isotypic solid...

C - Chemistry – Metallurgy – 30 – B

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148/3.6

C30B 9/12 (2006.01) C30B 9/00 (2006.01)

Patent

CA 1304275

A B R E G E SYNTHESES EN FLUX DE CRISTAUX ET EPITAXIES DE SOLUTIONS SOLIDES ISOTYPES DE KTiOPO4. La synthèse en flux de KTP et de ses isotypes de formule KaRb1-a TiOPbAs1-bO4 comprend : - l'utilisation comme flux des hydroxydes de potassium et de rubidium, - le chauffage à une température de 600 à 800° C pendant 25 à 100 heures environ avec un gradient thermique de 5 à 25° C/cm, - l'introduction d'un germe dans la solution à proximité de sa surface, puis le maintien de la température de palier ou le refroidissement de 1 à 5° C par heure. pas de figure

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