Device for coupling a micro-chromatograph with a mass...

G - Physics – 01 – N

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Details

G01N 30/72 (2006.01) G01N 30/88 (2006.01) G01N 30/30 (2006.01) H01J 49/04 (2006.01)

Patent

CA 2397898

The invention concerns a coupling device connecting a micro-chromatograph ( mu CG) output to a mass spectrometer input, said device comprising a capillary tube whereof one end is sealingly connected to the mass spectrometer vacuum source via an interface device, and whereof the other end is loosely connected to the micro-chromatograph output open to the atmosphere; the length and the diameter of the capillary tube being selected so that the flow rate inside the capillary tube is very close to the flow rate at the micro-chromatograph output; the interface device being further provided with heating means for adjusting very accurately the flow rate tapped by the capillary tube.

Dispositif de couplage reliant la sortie d'un microchromatographe (à) à l'entrée d'un spectromètre de masse (SM), ledit dispositif de couplage comprenant un tube capillaire dont l'une des extrémités est raccordée de façon étanche à la source sous vide du spectromètre de masse par l'intermédiaire d'un dispositif d'interface, et dont l'autre extrémité est raccordée à la sortie du microchromatographe, de manière lâche, ouverte sur l'atmosphère ; la longueur et le diamètre du tube capillaire étant choisis pour que le débit à l'intérieur du tube capillaire soit très voisin du débit à la sortie du microchromatographe; le dispositif d'interface étant, en outre, muni de moyens de chauffage pour ajuster très précisément le débit prélevé par le capillaire.

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