Electrocatalytic asymmetric dihydroxylation of olefinic...

Details Electrocatalytic asymmetric dihydroxylation of olefinic... Electrocatalytic asymmetric dihydroxylation of olefinic...

C - Chemistry, Metallurgy

25

B

C25B 3/02 (2006.01) B01J 31/16 (2006.01) B01J 31/40 (2006.01) B01J 37/34 (2006.01) C07C 29/48 (2006.01)

Patent

CA 2130564

A process is disclosed in with optically active glycols are produced through an electrolytic asymmetric dihydroxylation (ADH) reaction involving olefins as substrates. The ADH reaction is mediated by a catalytically active amount of osmium tetroxide or osmium-containing precursor in a profit medium in the presence of chiral ligand. Any lower valent osmium species produced in the course of the ADH reaction is regnerated electrolytically either directly in the absence of a secondary oxidant or indirectly in the presence of a secondary oxidant that itself undergoes electrolytic regeneration.

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