Electrochemical synthesis of niacin and other n-heterocyclic...

Details Electrochemical synthesis of niacin and other n-heterocyclic... Electrochemical synthesis of niacin and other n-heterocyclic...

C - Chemistry, Metallurgy

25

B

C25B 3/02 (2006.01) C07D 213/50 (2006.01) C07D 213/803 (2006.01) C07D 215/48 (2006.01)

Patent

CA 2043698

ABSTRACT An electrochemical oxidation of a pi-deficient N-heterocyclic precursor compound having an oxidizable organic group attached by a carbon-to-carbon linkage. This precursor compound is at least sparingly water soluble. The preferred electro-oxidation is conducted at an effective anode and in a medium which consists essentially of water, carboxylic acid, and the precursor compound. Preferred are electro-oxidations of substituted pyridine and quinoline bases and a particularly preferred aspect provides a convenient electrochemical synthesis of niacin from 3-methylpyridine.

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