Ester synthesis

C - Chemistry – Metallurgy – 07 – C

Patent

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Details

C07C 69/14 (2006.01) C07C 67/04 (2006.01)

Patent

CA 2182558

This invention relates to a process for the production of lower aliphatic esters by reacting a lower olefin with a saturated lower aliphatic mono- carboxylic acid in the vapour phase in the presence of a heteropolyacid catalyst characterised in that an amount of water in the range from 1-10 mole % based on the total of the olefin, aliphatic mono-carboxylic acid and water is added to the reaction mixture during the reaction. The presence of water enhances the yield of the desired ester. The reaction mixture may optionally contain a di-ether to minimise the by- products. The process is particularly suitable for producing ethyl acetate from ethylene and acetic acid in the presence of water.

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