Heat exchanging, optically interrogated chemical reaction...

G - Physics – 01 – N

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Details

G01N 1/31 (2006.01) B01J 19/00 (2006.01) B01L 3/00 (2006.01) B01L 7/00 (2006.01) F28F 3/12 (2006.01) F28F 21/04 (2006.01) G01N 21/03 (2006.01) G01N 35/00 (2006.01)

Patent

CA 2282623

The present invention provides a reaction vessel and apparatus for performing heat-exchanging reactions. The vessel has a chamber for holding a sample, the chamber being defined by two opposing major walls and a plurality of minor walls joining the major walls to each other, at least two of the walls being light transmissive to provide optical windows to the chamber. The apparatus comprises at least one heating surface for contacting at least one of the major walls, a heat source for heating the surface, and optics positioned to optically interrogate the chamber while the heating surface is in contact with at least one of the major walls. The optics include at least one light source for transmitting light to the chamber through a first one of the light transmissive walls and at least one detector for detecting light exiting the chamber through a second one of the light transmissive walls.

Cette invention se rapporte à un ensemble conçu pour la mise en oeuvre de réactions avec échange thermique régulé. Ledit ensemble comporte une chambre pour réaction chimique conçue pour recevoir un échantillon et permettre à ce dernier de réagir chimiquement; un manchon thermique muni d'éléments chauffants conçus pour entrer en contact thermique efficace avec une chambre réactionnelle; un instrument ayant un logement comportant une connexion électrique, une source de refroidissement, une zone de traitement conçue pour recevoir un manchon thermique, et un ensemble optique en communication optique avec une chambre pour réaction chimique; et un circuit de contrôle et de commande de l'ensemble optique, conçu pour recevoir le signal de sortie de l'ensemble optique. De préférence, on dispose d'une pluralité de logements et de modules associés pouvant être, chacun, régulés automatiquement lors d'opérations avec échange thermique.

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