C - Chemistry – Metallurgy – 01 – B
Patent
C - Chemistry, Metallurgy
01
B
23/223
C01B 21/072 (2006.01) C04B 35/581 (2006.01)
Patent
CA 1334475
Methods are described for preparing aluminum nitride of controllable morphology for ceramic and heat conduction applications. The methods comprise forming spherical particles or flakes of an intermediate, RAlNH, followed by heating the spheres or flakes of RAlNH at elevated temperatures to produce high purity aluminum nitride of corresponding morphology. Spheres of RAlNH are formed by (i) freezing a suspension of RAlNH in a liquid medium and thawing, by (ii) aging the suspension, or by (iii) dissolving RAlNH in a liquid medium and precipitating it. Flakes are formed by freezing a suspension of RAlNH in a liquid medium and removing frozen liquid medium from the frozen suspension.
546037
Bolt John Davis
Mahler Walter
Tebbe Frederick Nye
Young Robert Joseph Jr.
E.i. Du Pont de Nemours And Company
Sim & Mcburney
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