Improved methods of making cross-bridged macropolycycles

Details Improved methods of making cross-bridged macropolycycles Improved methods of making cross-bridged macropolycycles

C - Chemistry, Metallurgy

07

F

C07F 13/00 (2006.01)

Patent

CA 2448261

The present invention is directed to a method for preparing a complex of manganese and a cross-bridged macropolycycle. The method comprises the steps of (A) forming a bisaminal from an acyclic amine; (B) forming a diquat derivative of said bisaminal; (C) reducing said diquat derivative; (D) separating reducing agent and solvent from the product step of (C) in one or more operations; (E) removing residual hydride from the product of (D); (F) isolating a cross- bridged tetraazamacrocycle product of steps (A)-(E); and (G) reacting the product of step (F) with a manganous containing compound, thereby forming a manganese complex.

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