Improved process for preparing isepamicin

Details Improved process for preparing isepamicin Improved process for preparing isepamicin

C - Chemistry, Metallurgy

07

H

C07H 15/236 (2006.01) C07C 233/47 (2006.01) C07D 277/74 (2006.01) C07H 15/26 (2006.01)

Patent

CA 2062788

An improved process for converting gentamicin B to isepamicin comprising forming 3,6'-di-N-formylgentamicin B, acylat- ing the l-amino group with an N-protected (S)-isoserine compound and removing all the blocking groups under conditions which result in high yields of isepamicin. A novel formylating agent, 2- formylmercaptobenzothiazole, and intermediate compounds are also disclosed.

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