Improved process for the purification and recovery of...

C - Chemistry – Metallurgy – 07 – C

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C07C 253/34 (2006.01) C07C 253/24 (2006.01) C07C 253/26 (2006.01) C07C 255/03 (2006.01)

Patent

CA 2415395

A method for the purification of crude acetonitrile comprising distilling the crude acetonitrile in a first fractional distillation column at below atmospheric pressure, withdrawing a first side draw fraction comprising acetonitrile, distilling the first side draw fraction in a second fractional distillation column at super atmospheric pressure, and withdrawing from the second distillation a second side draw fraction comprising purified acetonitrile.

L'invention concerne un procédé de purification d'actéonitrile brut consistant à distiller l'acétonitrile brut dans une première colonne de distillation fractionnée à une pression inférieure à la pression atmosphérique, à retirer une première fraction soutirée latérale, à distiller ladite première fraction dans une seconde colonne de distillation fractionnée à une pression supérieure à la pression atmosphérique et à retirer de la seconde distillation une seconde fraction soutirée latérale renfermant l'acétonitrile purifié.

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