C - Chemistry – Metallurgy – 08 – F
Patent
C - Chemistry, Metallurgy
08
F
402/396, 23/431,
C08F 2/32 (2006.01) B01J 3/04 (2006.01) C08F 2/00 (2006.01) C08F 2/02 (2006.01)
Patent
CA 1136344
ABSTRACT OF THE DISCLOSURE This invention relates to a process of pro- ducing vinyl polymers by an inversion polymerization technique in the presence of a coating on the internal surfaces of the polymerization reactor. The coating on said surfaces may be a singular layer or a dual layer coating. By inversion polymerization is meant conduct- ing the initial stage of the polymerization reaction in a medium wherein the monomer or monomers being polymer- ized constitute the continuous phase and in the second or later stage of polymerization, water constitutes the continuous phase. The principal coating, or under- coating when a dual layer coating is employed, comprises protein, such as egg albumen, and when a top coating is used it comprises a water-soluble suspending agent, such as an alkyl or alkyl hydroxyalkyl cellulose ether. When polymerizing olefinic monomers, such as vinyl halides, vinylidene halides, and vinylidene monomers having at least one terminal CH2=C< grouping, and mixtures thereof, in the presence of said coating, polymer buildup on the inner surfaces of the reaction vessel is substantially eliminated. With the present invention, multiple charges or batches of polymer can be made in said internally coated reaction vessel without opening the same between charges, thus preventing the escape of unreacted monomer to the atmosphere.
345107
Goodrich (b.,f.) Company (the)
Sherman
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